Size Selective Synthesis of Tetraoctylammonium Bromide Stabilized/Nonstabilized Sulfur Nanoparticles
Article info
2015-06-11
2015-06-30
303 - 322
Keywords
- TEM
- XRD
- Sulfur.
- Stabilizer
- Nanoparticles
- Size selective synthesis
Abstract
Sulfur nanoparticles (S NPs) were prepared by a quick precipitation method in the absence and presence of tetraoctylammonium bromide (TOAB) that was used as a stabilizer to control the nanoparticles size. Scanning electron microscope (SEM), transmission electron microscope (TEM) and X-Ray Diffraction (XRD) were used to characterize the obtained S NPs. The average size of S NPs was in the range 2.4 – 8.9 nm, with spherical like shape. The NPs size was controlled by changing the preparation parameters: temperatures, different acid concentrations, different acid types and the presence of TOAB stabilizer.
Suleiman, M., Al Ali, A., Hussein, A., & Aref, D. (2016). Size Selective Synthesis of Tetraoctylammonium Bromide Stabilized/Nonstabilized Sulfur Nanoparticles. An-Najah University Journal for Research - A (Natural Sciences), 30(2), 303–322. https://doi.org/10.35552/anujr.a.30.2.1281
[1]M. Suleiman, A. Al Ali, A. Hussein, and D. Aref, “Size Selective Synthesis of Tetraoctylammonium Bromide Stabilized/Nonstabilized Sulfur Nanoparticles,” An-Najah University Journal for Research - A (Natural Sciences), vol. 30, no. 2, pp. 303–322, Jun. 2016, doi: 10.35552/anujr.a.30.2.1281.
Suleiman, Mohammed, et al. “Size Selective Synthesis of Tetraoctylammonium Bromide Stabilized/Nonstabilized Sulfur Nanoparticles.” An-Najah University Journal for Research - A (Natural Sciences), vol. 30, no. 2, June 2016, pp. 303–22. Crossref, https://doi.org/10.35552/anujr.a.30.2.1281.
1.Suleiman M, Al Ali A, Hussein A, Aref D. Size Selective Synthesis of Tetraoctylammonium Bromide Stabilized/Nonstabilized Sulfur Nanoparticles. An-Najah University Journal for Research - A (Natural Sciences) [Internet]. 2016 Jun;30(2):303–22. Available from: http://dx.doi.org/10.35552/anujr.a.30.2.1281
Suleiman, Mohammed, Anas Al Ali, Ayman Hussein, and Diaa Aref. “Size Selective Synthesis of Tetraoctylammonium Bromide Stabilized/Nonstabilized Sulfur Nanoparticles.” An-Najah University Journal for Research - A (Natural Sciences) 30, no. 2 (June 2016): 303–22. https://doi.org/10.35552/anujr.a.30.2.1281.
TOAB تحضير حبيبات نانومترية من الكبريت المثبت والغير مثبت بواسطة
المؤلفون:
معلومات المقال
2015-06-11
2015-06-30
303 - 322
الكلمات الإفتتاحية
- TEM
- XRD
- Sulfur.
- Stabilizer
- Nanoparticles
- Size selective synthesis
الملخص
تم في هذه الدراسة تحضير حبيبات الكبريت بحجم النانومتر وبشكل كروي وبعدة احجام مختلفة وذلك عن طريق تفاعل ترسيب الكبريت على درجات حرارة مختلفة واستخدام تراكيز وانواع من احماض مختلقة تم ذلك بوجود وعدم وجود.TOAB المثبت السطحي تم تشخيص تم تشخيص العينات المحضرة باستخدام الاجهزة التالية: XRD, TEM , SEM. اظهرت النتائج ان حجم حبيبات الكبريت المحضرة يتراوح ما بين2.4-8.9 nm.
Suleiman, M., Al Ali, A., Hussein, A., & Aref, D. (2016). Size Selective Synthesis of Tetraoctylammonium Bromide Stabilized/Nonstabilized Sulfur Nanoparticles. An-Najah University Journal for Research - A (Natural Sciences), 30(2), 303–322. https://doi.org/10.35552/anujr.a.30.2.1281
[1]M. Suleiman, A. Al Ali, A. Hussein, and D. Aref, “Size Selective Synthesis of Tetraoctylammonium Bromide Stabilized/Nonstabilized Sulfur Nanoparticles,” An-Najah University Journal for Research - A (Natural Sciences), vol. 30, no. 2, pp. 303–322, Jun. 2016, doi: 10.35552/anujr.a.30.2.1281.
Suleiman, Mohammed, et al. “Size Selective Synthesis of Tetraoctylammonium Bromide Stabilized/Nonstabilized Sulfur Nanoparticles.” An-Najah University Journal for Research - A (Natural Sciences), vol. 30, no. 2, June 2016, pp. 303–22. Crossref, https://doi.org/10.35552/anujr.a.30.2.1281.
1.Suleiman M, Al Ali A, Hussein A, Aref D. Size Selective Synthesis of Tetraoctylammonium Bromide Stabilized/Nonstabilized Sulfur Nanoparticles. An-Najah University Journal for Research - A (Natural Sciences) [Internet]. 2016 Jun;30(2):303–22. Available from: http://dx.doi.org/10.35552/anujr.a.30.2.1281
Suleiman, Mohammed, Anas Al Ali, Ayman Hussein, and Diaa Aref. “Size Selective Synthesis of Tetraoctylammonium Bromide Stabilized/Nonstabilized Sulfur Nanoparticles.” An-Najah University Journal for Research - A (Natural Sciences) 30, no. 2 (June 2016): 303–22. https://doi.org/10.35552/anujr.a.30.2.1281.
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